Chemical Engineering(English) | |||||
Bachelor | TR-NQF-HE: Level 6 | QF-EHEA: First Cycle | EQF-LLL: Level 6 |
Course Code: | CHM214 | ||||
Course Name: | Organic Chemistry Laboratory II | ||||
Course Semester: | Spring | ||||
Course Credits: |
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Language of instruction: | |||||
Course Requirement: | |||||
Does the Course Require Work Experience?: | No | ||||
Type of course: | Necessary | ||||
Course Level: |
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Mode of Delivery: | Face to face | ||||
Course Coordinator : | Dr.Öğr.Üyesi GÜLŞAH YAMAN UZUNOĞLU | ||||
Course Lecturer(s): | Gülşah YAMAN UZUNOĞLU | ||||
Course Assistants: |
Course Objectives: | Main objective is to teach the fundamentals of organic chemistry, properties of functional groups and, evaluating the main chemical reactions. Main objective is to provide information about general tools used in organic chemistry, reaction systems, separation and purification methods, reaction design, setting up a chemical reaction, running a reaction and obtaining products. |
Course Content: | Introduction to organic chemistry, recognition and naming of functional groups, classification of organic compounds, their properties, preparation (synthesis) and reactions, spectral structure determination, qualitative determination. |
The students who have succeeded in this course;
1) Learning how to calculate a limiting reagent, yield, and percent yield 2) Learning how to maintain a detailed scientific notebook 3) Learning how to critically evaluate data collected to determine the identity, purity, and yield of products 4) Learning how to summarize findings in writing in a clear and concise manner 5) Having knowledge about general organic reaction set ups 6) Learning how to engage in safe laboratory practices handling laboratory glassware, equipment, and chemical reagents 7) Learning how to characterize organic molecules by qualitative analysis and physical and spectroscopic techniques including mp, bp, IR, NMR 8) Learning how to run organic reactions by applying appropriate methods 9) how to perform purification techniques, such as filtration, suction filtration and recrystallization. |
Week | Subject | Related Preparation |
1) | Introduction, General Information, Report Writing Rules | -Organik Kimya Laboratuvar El Kitabı |
2) | Synthesis of tert-butyl chloride | -Organik Kimya Laboratuvar El Kitabı -Deneyde kullanılan kimyasalların fiziksel ve kimyasal özellikleri hakkında araştırma |
3) | Synthesis of acetanilide | -Organik Kimya Laboratuvar El Kitabı -Deneyde kullanılan kimyasalların fiziksel ve kimyasal özellikleri hakkında araştırma |
4) | Synthesis of p-nitroacetanilide | -Organic Chemistry I & II Laboratory Manual -Research about the physical and chemical properties of chemicals used in this experiment. |
5) | Synthesis of p-nitroaniline | -Organic Chemistry I & II Laboratory Manual -Research about the physical and chemical properties of chemicals used in this experiment. |
6) | Synthesis of phenylazo betanapthol | -Organic Chemistry I & II Laboratory Manual -Research about the physical and chemical properties of chemicals used in this experiment. |
7) | General review | -Organic Chemistry I & II Laboratory Manual -Ders notları Laboratory notebook |
8) | Midterm | -Organic Chemistry I & II Laboratory Manual -Lecture notes on reactions and properties of compounds used and synthesized -Laboratory notebook |
9) | Synthesis of benzylic acid | -Organic Chemistry I & II Laboratory Manual -Research about the physical and chemical properties of chemicals used in this experiment. |
10) | Synthesis of benzylidene aniline | -Organic Chemistry I & II Laboratory Manual -Research about the physical and chemical properties of chemicals used in this experiment. |
11) | Organic Structure Analysis- Degree of unsaturation, FTIR Spectroscopy | -Organic Chemistry Laboratory I&II Manual -Lecture notes -Chapter 13 (Structure Determination) in the textbook "John McMurry, Fundamentals of Organic Chemistry, Cornell University, 7th Edition". |
12) | Organic Structure Analysis- Mass Spectroscopy, NMR Spectroscopy | -Organic Chemistry Laboratory I&II Manual -Lecture notes -Chapter 13 (Structure Determination) in the textbook "John McMurry, Fundamentals of Organic Chemistry, Cornell University, 7th Edition". |
13) | Make up | -Organic Chemistry I & II Laboratory Manual -Research about the physical and chemical properties of chemicals used in this experiment. |
14) | General Review | -Organic Chemistry Laboratory I&II Manual -Lecture notes -Laboratory notebook |
Course Notes / Textbooks: | -Yaman Uzunoğlu, Gülşah, Organic Chemistry I & II Laboratory Manual, 2023, Istanbul Health and Technology University. -Lecture notes |
References: | 1. Jerry R. Mohrig, David G. Alberg, Gretchen E. Hofmeister, Paul F. Schatz, Christina Noring Hammond, “Laboratory Techniques in Organic Chemistry”, 4th Edition, W. H. Freeman and Company, 2014. 2. Louis F. Fieser, Kenneth L. Williamson, “Organic Experiments”, 7th Edition, Heath and Company, 1992. 3. Keller, Lichter, San Miguel, “Organic Chemistry 1 and 2 Laboratory Manual”, 4th Edition, 4. Linda Paar, Jeffrey Elbert, Kirk Manfredi, “Organic Chemistry Laboratory Experiments for Organic Chemistry Laboratory 861-121”. 5. Williamson, K. E. Macroscale and Microscale Organic Chemistry Experiments , 4th ed., Houghton Mifflin, Boston, 2003. 6. Hilal Çam, Levent Artok, Hüseyin Gözener, Hatice Güllübağ, Organic Chemistry Laboratory Manual, İzmir Institute of Technology. 7. Nichols, Lisa, “Organic Chemistry laboratory Techniques”, 2nd Edition. 8. Gamze Özgül Artuç, “Organik Kimya Laboratuvar Föyü”, İstanbul Sağlık ve Teknoloji Üniversitesi, 2022. 9. Qualitative Analysis of Organic Compounds, Ankara University (https://acikders.ankara.edu.tr/pluginfile.php/124521/mod_resource/content/0/Functional%20group%20analysis.pdf) |
No Effect | 1 Lowest | 2 Medium | 3 Highest |
Program Outcomes | Level of Contribution | |
1) | To be able to use advanced theoretical and practical knowledge acquired in the field | |
2) | To be able to interpret and evaluate data using advanced knowledge and skills acquired in the field, to be able to identify and analyze problems, to be able to develop solutions based on research and evidence. | |
3) | To be able to plan and manage activities for the development of employees under his/her responsibility within the framework of a project. | |
4) | To act in accordance with social, scientific, cultural and ethical values in the stages of collecting, interpreting, applying and announcing the results of data related to the field. | |
5) | To be able to carry out an advanced level study related to the field independently. | |
6) | To be able to take responsibility individually and as a team member to solve complex and unforeseen problems encountered in applications related to the field. | |
7) | To have advanced theoretical and practical knowledge supported by textbooks, application tools and other resources containing up-to-date information in the field. | |
8) | To have sufficient awareness of the universality of social rights, social justice, quality culture and protection of cultural values, environmental protection, occupational health and safety. | |
9) | To be able to inform the relevant people and institutions about the issues related to the field; to be able to convey his / her thoughts and suggestions for solutions to problems in written and orally. | |
10) | To be able to share his/her thoughts and suggestions for solutions to problems related to his/her field with experts and non-experts by supporting them with quantitative and qualitative data. | |
11) | To be able to organize and implement projects and activities for the social environment in which he/she lives with a sense of social responsibility | |
12) | To be able to evaluate the advanced knowledge and skills acquired in the field with a critical approach | |
13) | To be able to identify their learning needs and direct their learning |
Yazılı Sınav (Açık uçlu sorular, çoktan seçmeli, doğru yanlış, eşleştirme, boşluk doldurma, sıralama) | |
Homework | |
Uygulama | |
Gözlem | |
Raporlama |
Semester Requirements | Number of Activities | Level of Contribution |
Midterms | 1 | % 20 |
Final | 1 | % 40 |
Paper Submission | 7 | % 40 |
total | % 100 | |
PERCENTAGE OF SEMESTER WORK | % 60 | |
PERCENTAGE OF FINAL WORK | % 40 | |
total | % 100 |
Activities | Number of Activities | Aktiviteye Hazırlık | Aktivitede Harçanan Süre | Aktivite Gereksinimi İçin Süre | Workload | ||
Course Hours | 0 | 2 | 0 | ||||
Laboratory | 14 | 2 | 28 | ||||
Study Hours Out of Class | 14 | 1 | 14 | ||||
Midterms | 1 | 1 | 1 | ||||
Paper Submission | 7 | 2 | 14 | ||||
Final | 1 | 1 | 1 | ||||
Total Workload | 58 |